there likely is a layer of liquid water. Deprotonation of the amide proton caused a large variation of the 19F chemical shift. The pKa of the probe was modulated by varying the substituents on the aromatic group and an optimal value of 7.1 was obtained with an ortho cyano substituent. The introduction of phosphinate pendant arms allowed narrower linewidths and faster longitudinal relaxation rates to be achieved.
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